C₅₈H₉₆O₉Si₃

Base Information

Chemical Name:C₅₈H₉₆O₉Si₃
CAS No.:1268269-26-6
Molecular Formula:C₅₈H₉₆O₉Si₃
Molecular Weight:1021.65
Hs Code.:

C<sub>58</sub>H<sub>96</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₅₈H₉₆O₉Si₃

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Chemical Property of C₅₈H₉₆O₉Si₃

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Technology Process of C₅₈H₉₆O₉Si₃

There total 23 articles about C₅₈H₉₆O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 924656-70-2
C₅₈H₉₈O₉Si₃

: 1268269-26-6
C₅₈H₉₆O₉Si₃

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dichloromethane; dimethyl sulfoxide; at 0 - 20 ℃;
DOI:10.1021/ol900769d

Reference yield:

: 924656-50-8
C₇₀H₁₁₆O₁₀Si₄

: 1268269-26-6
C₅₈H₉₆O₉Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: zinc trifluoromethanesulfonate / dichloromethane / 20 °C / Inert atmosphere

2: 2,6-dimethylpyridine / dichloromethane / 6 h / Inert atmosphere

3: zinc trifluoromethanesulfonate / n-heptane; dichloromethane / 0 - 20 °C / Inert atmosphere

4: 4,4'-di-tert-butylbiphenyl; lithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

5: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; 4,4'-di-tert-butylbiphenyl; sulfur trioxide pyridine complex; lithium; zinc trifluoromethanesulfonate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; n-heptane; dichloromethane; 5: Parikh-Doering oxidation;
DOI:10.1021/ja200089f

Reference yield:

: 924656-53-1
C₆₅H₁₀₄O₉Si₃

: 1268269-26-6
C₅₈H₉₆O₉Si₃

Guidance literature:: Multi-step reaction with 2 steps

1: 4,4'-di-tert-butylbiphenyl; lithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With 4,4'-di-tert-butylbiphenyl; sulfur trioxide pyridine complex; lithium; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 2: Parikh-Doering oxidation;
DOI:10.1021/ja200089f