(E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

Base Information

Chemical Name:(E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene
CAS No.:1422985-10-1
Molecular Formula:C₁₀H₅F₆NO₂
Molecular Weight:285.146
Hs Code.:

Synonyms:(E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

Suppliers and Price of (E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

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Technology Process of (E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

There total 1 articles about (E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74853-66-0
4'-trifluoromethyl-2,2,2-trifluoroacetophenone

: 1422985-10-1
(E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / 20 °C

2: thionyl chloride; pyridine / toluene / 3 h / 0 - 20 °C

With pyridine; thionyl chloride; triethylamine; In toluene; 1: |Henry Nitro Aldol Condensation;
DOI:10.1021/ja400650m

Reference yield: 90.0%

: 1374605-89-6
tert-butyl 2-oxo-3-(propan-2-ylidene)indoline-1-carboxylate

: 1422985-10-1
(E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

: 1570104-91-4
(R,Z)-tert-butyl 2-oxo-3-(5,5,5-trifluoro-4-(nitromethyl)-4-(4-(trifluoromethyl)phenyl)pentan-2-ylidene)indoline-1-carboxylate

Guidance literature:: With C₂₉H₂₈F₆N₄OS; In toluene; at 20 ℃; for 36h; enantioselective reaction;
DOI:10.1021/ol500157b

Reference yield: 80.0%

: 120-72-9
indole

: 1422985-10-1
(E)-1-(3,3,3-trifluoro-1-nitroprop-1-en-2-yl)-4-(trifluoromethyl)benzene

: 1422985-29-2
3-(1,1,1-trifluoro-3-nitro-2-(4-(trifluoromethyl)phenyl)propan-2-yl)-1H-indole

Guidance literature:: With nickel(II) perchlorate hexahydrate; 2,2-bis<2-<4(R),5(R)-diphenyl-1,3-oxazolinyl>>propane; In toluene; at 60 ℃; enantioselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1021/ja400650m