(Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

Base Information

Chemical Name:(Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate
CAS No.:1035695-41-0
Molecular Formula:C₃₇H₄₆N₂O₉
Molecular Weight:662.78
Hs Code.:

Synonyms:(Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

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Chemical Property of (Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

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Technology Process of (Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

There total 1 articles about (Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: (Z)-isopropyl 3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

: 100-39-0
benzyl bromide

: 1035695-41-0
(Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.1021/jo800898k

Reference yield: 70.0%

: 1035695-41-0
(Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

: (E)-3-benzyl-2-[(2,4,5-trimethoxy-3-methylphenyl)methylene]-7,9,10-trimethoxy-8-methyl-4-oxo-1,2,3,4,5,6-hexahydro-1,5-imino-3-benzazocine-11-carboxylic acid isopropyl ester

Guidance literature:: With N-Bromosuccinimide; In acetonitrile; at 60 ℃; for 0.25h;
DOI:10.1021/jo800898k

Reference yield: 25.0%

: 1035695-41-0
(Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate

: 113479-98-4
(Z)-4-benzyl-1-<(isopropyloxy)carbonyl>-6-<2,4,5-trimethoxy-3-methylphenyl)methyl>-3-<(2,4,5-trimethoxy-3-methylphenyl)methylene>-2,5-piperazinedione

: (E)-3-benzyl-2-[(2,4,5-trimethoxy-3-methylphenyl)methylene]-7,9,10-trimethoxy-8-methyl-4-oxo-1,2,3,4,5,6-hexahydro-1,5-imino-3-benzazocine-11-carboxylic acid isopropyl ester

Guidance literature:: (Z)-isopropyl 4-benzyl-3-oxo-(2,4,5-trimethoxy-3-methylbenzyl)-5-(2,4,5-trimethoxy-3-methylbenzylidene)piperazine-1-carboxylate; With ammonium cerium(IV) nitrate; In methanol; at 20 ℃; for 1h;

With formic acid; at 60 ℃; for 1h; Further stages.;
DOI:10.1021/jo800898k