2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

Base Information

Chemical Name:2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid
CAS No.:198416-01-2
Molecular Formula:C₁₇H₂₄N₂O₆
Molecular Weight:352.387
Hs Code.:

Synonyms:2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

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Chemical Property of 2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

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Technology Process of 2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

There total 2 articles about 2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 198416-00-1
3-amino-2-(N-benzyloxycarbonyl-N-methyl)aminopropionic acid

: 198416-01-2
2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

Guidance literature:: With sodium hydroxide;
DOI:10.1021/ja972670j

Reference yield:

: 2-(Benzyloxycarbonyl-methyl-amino)-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionic acid tert-butyl ester

: 198416-01-2
2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 1.) N₂H₄, 2.) CF₃COOH

2: 32 percent / aq. NaOH

With sodium hydroxide; trifluoroacetic acid; hydrazine;
DOI:10.1021/ja972670j

Reference yield: 41.0%

: 198416-02-3
(2-Methyl-isothioureidocarbonyl)-carbamic acid benzyl ester

: 198416-01-2
2-(N-benzyloxycarbonyl-N-methyl)amino-3-(tert-butoxycarbonylamino)propionic acid

: 198416-03-4
[3-(3-Benzyloxycarbonylaminocarbonyl-2-methyl-isothioureido)-2-(benzyloxycarbonyl-methyl-amino)-3-oxo-propyl]-carbamic acid tert-butyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Ambient temperature;
DOI:10.1021/ja972670j