3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide

Base Information

• Chemical Name: 3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide
• CAS No.: 1035695-38-5
• Molecular Formula: C₂₆H₃₄N₂O₇
• Molecular Weight: 486.565

Synonyms:3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide

Chemical Property of 3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide

Chemical Property:

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Technology Process of 3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide

There total 1 articles about 3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

3-(2,4,5-trimethoxy-3-methylphenyl)propiolaldehyde (1035695-31-8) + C13H20N2O4 → 3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide (1035695-38-5)

Guidance literature:

3-(2,4,5-trimethoxy-3-methylphenyl)propiolaldehyde; C₁₃H₂₀N₂O₄; In methanol; at 20 ℃; for 0.5h;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃; Further stages.;

DOI:10.1021/jo800898k

Reference yield: 88.0%

3-(2,4,5-trimethoxy-3-methylphenyl)-2-(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynylamino)propanamide (1035695-38-5) + isopropyl chloroformate (108-23-6) → isopropyl 1-amino-1-oxo-3-(2,4,5-trimethoxy-3-methylphenyl)propan-2-yl(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynyl)carbamate (1035695-39-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 6h;

DOI:10.1021/jo800898k

upstream raw materials:

3-(2,4,5-trimethoxy-3-methylphenyl)propiolaldehyde

Downstream raw materials:

isopropyl 1-amino-1-oxo-3-(2,4,5-trimethoxy-3-methylphenyl)propan-2-yl(3-(2,4,5-trimethoxy-3-methylphenyl)prop-2-ynyl)carbamate

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