2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

Base Information

Chemical Name:2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid
CAS No.:1394134-85-0
Molecular Formula:C₂₂H₁₄BrNO₅
Molecular Weight:452.261
Hs Code.:

Synonyms:2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

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Chemical Property of 2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

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Technology Process of 2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

There total 3 articles about 2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394134-84-9
2-((3-bromo-4-hydroxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

: 74-88-4
methyl iodide

: 1394134-85-0
2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

Guidance literature:: With silver(l) oxide; In chloroform; at 20 ℃; for 40h; Darkness;
DOI:10.1016/j.bmc.2012.06.002

Reference yield:

: 129-43-1
1-hydroxyanthraquinone

: 1394134-85-0
2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: bromine; sodium acetate; acetic acid / 16 h / Reflux

2.1: potassium acetate; copper diacetate; copper / pentan-1-ol / 150 - 160 °C

2.2: 0.17 h / 80 - 90 °C

3.1: silver(l) oxide / chloroform / 40 h / 20 °C / Darkness

With bromine; potassium acetate; copper diacetate; sodium acetate; copper; acetic acid; silver(l) oxide; In pentan-1-ol; chloroform;
DOI:10.1016/j.bmc.2012.06.002

Reference yield:

: 52146-83-5
2,4-dibromo-1-hydroxyanthracene-9,10-dione

: 1394134-85-0
2-((3-bromo-4-methoxy-9,10-dioxo-9,10-dihydroanthracen-1-yl)amino)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium acetate; copper diacetate; copper / pentan-1-ol / 150 - 160 °C

1.2: 0.17 h / 80 - 90 °C

2.1: silver(l) oxide / chloroform / 40 h / 20 °C / Darkness

With potassium acetate; copper diacetate; copper; silver(l) oxide; In pentan-1-ol; chloroform;
DOI:10.1016/j.bmc.2012.06.002