5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione

Base Information

• Chemical Name: 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione
• CAS No.: 623936-95-8
• Molecular Formula: C₂₂H₁₈ClN₅O₅S
• Molecular Weight: 499.934

Synonyms:5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione

Chemical Property of 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione

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Technology Process of 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione

There total 1 articles about 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-(4-chloro-3-methylphenoxymethyl)-4-amino-5-mercapto-1,2,4-triazole (118794-57-3) + 5-(4-methoxy-2-nitrophenyl)furan-2-carbaldehyde (415943-88-3) → 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione (623936-95-8)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; ethanol; for 4h; Heating;

DOI:10.1016/S0223-5234(03)00128-4

Reference yield: 80.0%

morpholine (110-91-8,99108-56-2) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione (623936-95-8) → 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2-morpholin-4-ylmethyl-2,4-dihydro-[1,2,4]triazole-3-thione

Guidance literature:

In 1,4-dioxane; ethanol; at 20 ℃;

DOI:10.1016/S0223-5234(03)00128-4

Reference yield: 74.0%

1-methyl-piperazine (109-01-3) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2,4-dihydro-[1,2,4]triazole-3-thione (623936-95-8) → 5-(4-Chloro-3-methyl-phenoxymethyl)-4-{[1-[5-(4-methoxy-2-nitro-phenyl)-furan-2-yl]-meth-(E)-ylidene]-amino}-2-(4-methyl-piperazin-1-ylmethyl)-2,4-dihydro-[1,2,4]triazole-3-thione

Guidance literature:

In 1,4-dioxane; ethanol; at 20 ℃;

DOI:10.1016/S0223-5234(03)00128-4

upstream raw materials:

3-(4-chloro-3-methylphenoxymethyl)-4-amino-5-mercapto-1,2,4-triazole

5-(4-methoxy-2-nitrophenyl)furan-2-carbaldehyde

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