pentabromobenzyl ester of ethoxycarbonylacetic acid

Base Information

• Chemical Name: pentabromobenzyl ester of ethoxycarbonylacetic acid
• CAS No.: 86808-70-0
• Molecular Formula: C₁₂H₉Br₅O₄
• Molecular Weight: 616.721

Synonyms:pentabromobenzyl ester of ethoxycarbonylacetic acid

Chemical Property of pentabromobenzyl ester of ethoxycarbonylacetic acid

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of pentabromobenzyl ester of ethoxycarbonylacetic acid

There total 2 articles about pentabromobenzyl ester of ethoxycarbonylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,3,4,5,6-pentabromobenzyl bromide (38521-51-6) + sodium diethylmalonate (996-82-7) → pentabromobenzyl ester of ethoxycarbonylacetic acid (86808-70-0)

Guidance literature:

In ethanol; at 78 ℃; for 4.4h;

DOI:10.1023/A:1012474416163

Reference yield:

2,3,4,5,6-pentabromobenzyl bromide (38521-51-6) + diethyl malonate (105-53-3) → pentabromobenzyl ester of ethoxycarbonylacetic acid (86808-70-0)

Guidance literature:

With sodium; Yield given. Multistep reaction; 1.) ethanol; 2.) reflux, 6 h;

Reference yield: 85.0%

pentabromobenzyl ester of ethoxycarbonylacetic acid (86808-70-0) → 2,3,4,5,6-pentabromobenzyl alcohol (79415-41-1)

Guidance literature:

With sulfuric acid; for 4h;

upstream raw materials:

2,3,4,5,6-pentabromobenzyl bromide

diethyl malonate

sodium diethylmalonate

Downstream raw materials:

2,3,4,5,6-pentabromobenzyl alcohol

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