hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

Base Information

Chemical Name:hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester
CAS No.:458567-80-1
Molecular Formula:C₂₁H₂₉NO₄
Molecular Weight:359.466
Hs Code.:

hex-5-enoic acid 2-[(allyl-<i>tert</i>-butoxycarbonyl-amino)-methyl]-phenyl ester

Synonyms:hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

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Chemical Property of hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

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Technology Process of hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

There total 3 articles about hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1577-22-6
5-hexenoic acid

: 458568-14-4
allyl-(2-hydroxy-benzyl)-carbamic acid tert-butyl ester

: 458567-80-1
hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 15h;
DOI:10.1021/ol0261579

Reference yield:

: 177780-96-0
2-[N-(prop-2'-enyl)aminomethyl]phenol

: 458567-80-1
hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CH₂Cl₂ / 15 h / 20 °C

2: 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 15 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1021/ol0261579

Reference yield:

: 90-02-8
salicylaldehyde

: 458567-80-1
hex-5-enoic acid 2-[(allyl-tert-butoxycarbonyl-amino)-methyl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium sulfate / tetrahydrofuran / 2 h / 20 °C

1.2: 95 percent / sodium triacetoxyborohydride / tetrahydrofuran / 15 h

2.1: 100 percent / CH₂Cl₂ / 15 h / 20 °C

3.1: 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 15 h / 20 °C

With dmap; sodium sulfate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0261579