(S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

Base Information

Chemical Name:(S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate
CAS No.:1007881-94-8
Molecular Formula:C₂₄H₂₈N₄O₄
Molecular Weight:436.511
Hs Code.:

Synonyms:(S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

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Chemical Property of (S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

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Technology Process of (S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

There total 4 articles about (S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 936242-42-1
(S)-2-((tert-butoxycarbonyl)amino)-4-pentynoic acid benzyl ester

: 100-39-0
benzyl bromide

: 1007881-94-8
(S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

Guidance literature:: With sodium azide; copper(II) sulfate; In water; N,N-dimethyl-formamide; at 20 - 65 ℃; for 17h;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1007881-94-8
(S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C

2: sodium azide / sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / 17 h / 65 °C

With dmap; sodium azide; N-ethyl-N,N-diisopropylamine; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 61172-66-5,63039-46-3,63039-48-5,143979-37-7
(S)-2-(tert-butoxycarbonylamino)pent-4-ynoic acid

: 1007881-94-8
(S)-benzyl 3-(1-benzyl-1H-1,2,3-triazol-4-yl)-2-(tert-butoxycarbonylamino)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C

2: sodium azide / sodium L-ascorbate; copper(ll) sulfate pentahydrate / N,N-dimethyl-formamide; water / 17 h / 65 °C

With dmap; sodium azide; N-ethyl-N,N-diisopropylamine; copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; N,N-dimethyl-formamide;