potassium 18-crown-6 fluoro(dimesityl)phenylborate

Base Information

• Chemical Name: potassium 18-crown-6 fluoro(dimesityl)phenylborate
• CAS No.: 1019996-67-8
• Molecular Formula: C₁₂H₂₄O₆*C₂₄H₂₇BF*K
• Molecular Weight: 648.705

Synonyms:potassium 18-crown-6 fluoro(dimesityl)phenylborate

Chemical Property of potassium 18-crown-6 fluoro(dimesityl)phenylborate

Chemical Property:

Purity/Quality:

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Technology Process of potassium 18-crown-6 fluoro(dimesityl)phenylborate

There total 5 articles about potassium 18-crown-6 fluoro(dimesityl)phenylborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimesityl(phenyl)borane (65881-97-2) + 18-crown-6 ether (17455-13-9) → potassium 18-crown-6 fluoro(dimesityl)phenylborate (1019996-67-8)

Guidance literature:

With potassium fluoride; In toluene; at 20 ℃; for 3.5h;

DOI:10.1021/ja710615r

Reference yield:

dimesityl(phenyl)borane (65881-97-2) + K(C4H8O)(CH2CH2O)6F2Si(CH3)2C6H4B(C6H2(CH3)3)2 → o-(fluorodimethylsilyl)(dimesitylboryl)benzene (1019996-49-6) + potassium 18-crown-6 fluoro(dimesityl)phenylborate (1019996-67-8)

Guidance literature:

In not given;

DOI:10.1021/ja710615r

Reference yield:

dimesityl(phenyl)borane (65881-97-2) + K(1+)*(CH2CH2O)6*2C4H8O*SiF2(C6H5)2C6H4B(C6H2(CH3)3)2(1-)=K(CH2CH2O)6(C4H8O)2SiF2(C6H5)2C6H4B(C6H2C3H9)2 → o-(fluorodiphenylsilyl)(dimesitylboryl)benzene (1019996-52-1) + potassium 18-crown-6 fluoro(dimesityl)phenylborate (1019996-67-8)

Guidance literature:

In not given;

DOI:10.1021/ja710615r

upstream raw materials:

dimesityl(phenyl)borane

18-crown-6 ether

Downstream raw materials:

dimesityl(phenyl)borane

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