tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate

Base Information

Chemical Name:tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate
CAS No.:1096155-18-8
Molecular Formula:C₃₆H₆₉NO₆Si₃
Molecular Weight:696.203
Hs Code.:

Synonyms:tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate

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Chemical Property of tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate

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Technology Process of tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate

There total 1 articles about tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 994-30-9
triethylsilyl chloride

: 1096155-31-5
tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-dihydroxy-5-(hydroxymethyl)pyrrolidine-1-carboxylate

: 1096155-18-8
tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1039/b815332a

Reference yield: 91.0%

: 1096155-18-8
tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate

: 1096155-14-4
tert-butyl (2R,3R,4R,5R)-2-(benzyloxymethyl)-5-formyl-3,4-bis(triethylsilyloxy)pyrrolidine-1-carboxylate

Guidance literature:: tert-butyl (2R,3R,4R,5S)-2-(benzyloxymethyl)-3,4-bis(triethylsilyloxy)-5-(triethylsilyloxymethyl)pyrrolidine-1-carboxylate; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 1.16667h; Inert atmosphere;

With triethylamine; at -78 - 20 ℃; for 1.16667h;
DOI:10.1039/b815332a