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11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol

Base Information Edit
  • Chemical Name:11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol
  • CAS No.:100311-71-5
  • Molecular Formula:C37H48O5Si
  • Molecular Weight:600.871
  • Hs Code.:
  • Mol file:100311-71-5.mol
11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol

Synonyms:11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol

Suppliers and Price of 11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol Edit
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Technology Process of 11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol

There total 6 articles about 11-O-benzoyl-3-O-(tert-butyldiphenylsilyl)-1,2-bis-O-(1-methylethylidene)-5-undecene-1,2(R),3(S),11-tetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1: lithium hexamethyldisilazane (LiHMDS) / tetrahydrofuran; hexamethylphosphoric acid triamide / 2.5 h / -78 - 20 °C
2: NaHCO3 / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / Ambient temperature
3: 68 percent / AlH3*Et2O / tetrahydrofuran / 0.5 h / 0 °C
4: 85 percent / Et3N / CH2Cl2 / 0 °C
With aluminium hydride * diethyl ether; sodium hydrogencarbonate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/jo00356a004
Guidance literature:
Multi-step reaction with 4 steps
1: lithium hexamethyldisilazane (LiHMDS) / tetrahydrofuran; hexamethylphosphoric acid triamide / 2.5 h / -78 - 20 °C
2: NaHCO3 / tetrahydrofuran; hexamethylphosphoric acid triamide / 2 h / Ambient temperature
3: 68 percent / AlH3*Et2O / tetrahydrofuran / 0.5 h / 0 °C
4: 85 percent / Et3N / CH2Cl2 / 0 °C
With aluminium hydride * diethyl ether; sodium hydrogencarbonate; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1021/jo00356a004
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