3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

Base Information

Chemical Name:3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride
CAS No.:73591-85-2
Molecular Formula:C₂₈H₂₉N₂O₇*Cl
Molecular Weight:541
Hs Code.:

Synonyms:3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

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Chemical Property of 3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

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Technology Process of 3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

There total 3 articles about 3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 73611-06-0
3,5-di-O-benzoyl-β-D-ribofuranosyl chloride

: 73591-72-7
5-isopropylnicotinamide

: 73591-85-2
3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

Guidance literature:: In acetonitrile; at -5 ℃; for 72h;
DOI:10.1016/0008-6215(80)90003-8

Reference yield:

: 42972-49-6
3-acetyl-5-isopropylpyridine

: 73591-85-2
3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / bromine/sodium hydroxide / H₂O / Ambient temperature

2: 61 percent / diethyl ether; methanol

3: 82 percent / ammonia / H₂O / 26 h / Ambient temperature

4: 89 percent / acetonitrile / 72 h / -5 °C

With sodium hydroxide; ammonia; bromine; In methanol; diethyl ether; water; acetonitrile;
DOI:10.1016/0008-6215(80)90003-8

Reference yield:

: 73591-69-2
5-isopropylnicotinic acid

: 73591-85-2
3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / diethyl ether; methanol

2: 82 percent / ammonia / H₂O / 26 h / Ambient temperature

3: 89 percent / acetonitrile / 72 h / -5 °C

With ammonia; In methanol; diethyl ether; water; acetonitrile;
DOI:10.1016/0008-6215(80)90003-8