3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI)

Base Information

• Chemical Name: 3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI)
• CAS No.: 73591-69-2
• Molecular Formula: C₉H₁₁NO₂
• Molecular Weight: 165.192
• Mol file: 73591-69-2.mol

Synonyms:3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI);5-ISOPROPYLNICOTINIC ACID

Chemical Property of 3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI)

Chemical Property:

• Vapor Pressure: 0.000219mmHg at 25°C
• Refractive Index: 1.538
• Boiling Point: 312.9°C at 760 mmHg
• PKA: 2.24±0.10(Predicted)
• Flash Point: 143°C
• PSA: 50.19000
• Density: 1.137g/cm³
• LogP: 1.90320
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

5-ISOPROPYLNICOTINIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI)

There total 1 articles about 3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-acetyl-5-isopropylpyridine (42972-49-6) → 5-isopropylnicotinic acid (73591-69-2)

Guidance literature:

With sodium hydroxide; bromine; In water; Ambient temperature;

DOI:10.1016/0008-6215(80)90003-8

Reference yield: 61.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 5-isopropylnicotinic acid (73591-69-2) → 5-isopropyl-3-methoxycarbonylpyridine (73591-71-6)

Guidance literature:

In methanol; diethyl ether;

DOI:10.1016/0008-6215(80)90003-8

Reference yield:

5-isopropylnicotinic acid (73591-69-2) → 3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride (73591-85-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 61 percent / diethyl ether; methanol

2: 82 percent / ammonia / H₂O / 26 h / Ambient temperature

3: 89 percent / acetonitrile / 72 h / -5 °C

With ammonia; In methanol; diethyl ether; water; acetonitrile;

DOI:10.1016/0008-6215(80)90003-8

upstream raw materials:

3-acetyl-5-isopropylpyridine

Downstream raw materials:

5-isopropyl-3-methoxycarbonylpyridine

3-carbamoyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-5-isopropylpyridinium chloride

5-isopropyl-1-(3,5-di-O-benzoyl-β-D-ribofuranosyl)-3-methoxycarbonylpyridinium chloride

5-isopropyl-1-(3,5-di-O-benzoyl-α-D-ribofuranosyl)-3-methoxycarbonylpyridinium chloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 73591-69-2 3-Pyridinecarboxylicacid,5-(1-methylethyl)-(9CI)

Send

Send

Metric Ton KG G Pound L ML

Send

Send