Technology Process of C15H22N6O2
There total 4 articles about C15H22N6O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / tetrahydrofuran / 16 h / 0 - 50 °C
2: tetrahydrofuran; methanol / 16 h / 0 - 20 °C
3: palladium on activated charcoal / N,N-dimethyl-formamide / 4 h / 20 °C
4: hydrogenchloride; tert.-butylnitrite; sodium azide / water
With
hydrogenchloride; sodium azide; tert.-butylnitrite; palladium on activated charcoal; potassium carbonate;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bbagen.2014.05.005
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran; methanol / 16 h / 0 - 20 °C
2: palladium on activated charcoal / N,N-dimethyl-formamide / 4 h / 20 °C
3: hydrogenchloride; tert.-butylnitrite; sodium azide / water
With
hydrogenchloride; sodium azide; tert.-butylnitrite; palladium on activated charcoal;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bbagen.2014.05.005
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium on activated charcoal / N,N-dimethyl-formamide / 4 h / 20 °C
2: hydrogenchloride; tert.-butylnitrite; sodium azide / water
With
hydrogenchloride; sodium azide; tert.-butylnitrite; palladium on activated charcoal;
In
water; N,N-dimethyl-formamide;
DOI:10.1016/j.bbagen.2014.05.005
