2-(Dicyclohexylphosphino)-1-phenylindole

Base Information

Chemical Name:2-(Dicyclohexylphosphino)-1-phenylindole
CAS No.:740815-36-5
Molecular Formula:C₂₆H₃₂NP
Molecular Weight:389.521
Hs Code.:29339900
European Community (EC) Number:815-232-5
DSSTox Substance ID:DTXSID70696510
Nikkaji Number:J2.124.256J
Wikidata:Q72502034
Mol file:740815-36-5.mol

Synonyms:740815-36-5;2-(DICYCLOHEXYLPHOSPHINO)-1-PHENYLINDOLE;2-(Dicyclohexylphosphino)-1-phenyl-1H-indole;N-Phenyl-2-(dicyclohexylphosphino)indol;dicyclohexyl-(1-phenylindol-2-yl)phosphane;2-(Dicyclohexylphosphanyl)-1-phenyl-1H-indole;C26H32NP;SCHEMBL2684525;DTXSID70696510;TZWPHBJJVRIXMS-UHFFFAOYSA-N;MFCD06798303;AKOS016012151;SC11202;BP-12238;N-phenyl-2-(dicyclohexyl-phosphino)indole;1-Phenyl-2-(dicyclohexylphosphino)-1H-indole;F87355;N-PHENYL-2-(DICYCLOHEXYLPHOSPHINO)INDOLE;2-(Dicyclohexylphosphino)-1-phenylindole, 95% (NMR);CATACXIUM(R) PINCY;N-PHENYL-2-(DICYCLOHEXYLPHOSPHINO)INDOL

Suppliers and Price of 2-(Dicyclohexylphosphino)-1-phenylindole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Strem Chemicals
N-Phenyl-2-(dicyclohexylphosphino)indol, min. 95% [cataCXium(R) PInCy]
500mg
$ 76.00

Strem Chemicals
N-Phenyl-2-(dicyclohexylphosphino)indol, min. 95% [cataCXium(R) PInCy]
2g
$ 228.00

Sigma-Aldrich
2-(Dicyclohexylphosphino)-1-phenylindole 95% (NMR)
1g
$ 200.00

Chemenu
dicyclohexyl-(1-phenylindol-2-yl)phosphane 95%+
1g
$ 391.00

American Custom Chemicals Corporation
2-(DICYCLOHEXYLPHOSPHINO)-1-PHENYLINDOLE 95.00%
5G
$ 1296.44

American Custom Chemicals Corporation
2-(DICYCLOHEXYLPHOSPHINO)-1-PHENYLINDOLE 95.00%
1MG
$ 597.89

Total 11 raw suppliers

Chemical Property of 2-(Dicyclohexylphosphino)-1-phenylindole

Chemical Property:

Melting Point:157-159℃ (hexane )
Boiling Point:546.2±32.0 °C(Predicted)
PSA：18.52000
LogP:7.40310
Sensitive.:air sensitive
XLogP3:7.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:389.227237023
Heavy Atom Count:28
Complexity:457

Purity/Quality:

95% ^*data from raw suppliers

N-Phenyl-2-(dicyclohexylphosphino)indol, min. 95% [cataCXium(R) PInCy] ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)P(C2CCCCC2)C3=CC4=CC=CC=C4N3C5=CC=CC=C5

Technology Process of 2-(Dicyclohexylphosphino)-1-phenylindole

There total 4 articles about 2-(Dicyclohexylphosphino)-1-phenylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 16096-33-6
1-phenyl-1H-indole

: 16523-54-9
chlorodicyclohexylphosphane

: 740815-36-5
2-(dicyclohexylphosphino)-N-phenylindole

Guidance literature:: 1-phenyl-1H-indole; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; toluene; at 100 ℃; for 3h;

chlorodicyclohexylphosphane; In hexane; toluene; at 100 ℃; for 2h;
DOI:10.1002/chem.200306026

Reference yield: 17.0%

: 16523-54-9
chlorodicyclohexylphosphane

: 740815-36-5
2-(dicyclohexylphosphino)-N-phenylindole

Guidance literature:: 1-phenyl-1H-indole; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In hexane; at 75 ℃; for 3h; Heating / reflux;

chlorodicyclohexylphosphane; In hexane; at 75 ℃; for 1h; Heating / reflux;

Reference yield:

: 120-72-9
indole

: 740815-36-5
2-(dicyclohexylphosphino)-N-phenylindole

Guidance literature:: Multi-step reaction with 2 steps

1.1: 85 percent / K₃PO₄; 1,2-diaminocyclohexane / CuI / dioxane / 24 h / 110 °C

2.1: n-BuLi; TMEDA / toluene; hexane / 3 h / 100 °C

2.2: 60 percent / toluene; hexane / 2 h / 100 °C

With potassium phosphate; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; rac-diaminocyclohexane; copper(l) iodide; In 1,4-dioxane; hexane; toluene;
DOI:10.1002/chem.200306026