(1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

Base Information

Chemical Name:(1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde
CAS No.:121772-23-4
Molecular Formula:C₁₅H₃₀O₃Si
Molecular Weight:286.487
Hs Code.:

Synonyms:(1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

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Chemical Property of (1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

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Technology Process of (1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

There total 6 articles about (1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 121772-22-3
[(1R,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexyl]-methanol

: 121772-23-4
(1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

Guidance literature:: With molecular sieve; pyridinium chlorochromate; In dichloromethane; Ambient temperature;
DOI:10.1002/hlca.19880710505

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 121772-23-4
(1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / (i-Pr)2NEt / CH₂Cl₂ / Ambient temperature

2: 91 percent / LiAlH₄ / tetrahydrofuran / 0 °C

3: 94 percent / pyridinium chlorochromate, molecular sieves / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; molecular sieve; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/hlca.19880710505

Reference yield:

: 121842-98-6
(2S,4aS,5S,8aS)-2-(tert-butyl)perhydro-4a,5-dimethyl-2H,4H-<1,3>benzodioxin-4-one

: 121772-23-4
(1S,2S,6S)-1,2-Dimethyl-6-(2-trimethylsilanyl-ethoxymethoxy)-cyclohexanecarbaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / LiOH / tetrahydrofuran; methanol; H₂O / Ambient temperature

2: 99 percent / diethyl ether / 0 °C

3: 98 percent / (i-Pr)2NEt / CH₂Cl₂ / Ambient temperature

4: 91 percent / LiAlH₄ / tetrahydrofuran / 0 °C

5: 94 percent / pyridinium chlorochromate, molecular sieves / CH₂Cl₂ / Ambient temperature

With lithium hydroxide; lithium aluminium tetrahydride; molecular sieve; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/hlca.19880710505