4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate

Base Information

• Chemical Name: 4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate
• CAS No.: 930785-30-1
• Molecular Formula: C₁₉H₂₅N₅O₅S
• Molecular Weight: 435.504

Synonyms:4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate

Chemical Property of 4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate

Chemical Property:

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Technology Process of 4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate

There total 2 articles about 4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-((6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl)phenyl)methanol (930294-00-1) → 4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate (930785-30-1)

Guidance literature:

With methanesulfonyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 1h;

Reference yield:

(4-((6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl)phenyl)methanol (930294-00-1) + methanesulfonyl chloride (124-63-0) → 4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate (930785-30-1)

Guidance literature:

With triethylamine; In 1-methyl-pyrrolidin-2-one; at 0 - 20 ℃;

Reference yield:

4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl methanesulfonate (930785-30-1) + methyl (3-{2-[methyl(piperidin-4-yl)amino]ethoxy}phenyl)acetate dihydrochloride → methyl (3-{2-[(1-{4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl}piperidin-4-yl)(methyl)amino]ethoxy}phenyl)acetate (930785-29-8)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

upstream raw materials:

(4-((6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl)phenyl)methanol

methanesulfonyl chloride

Downstream raw materials:

methyl (3-{2-[(1-{4-[(6-amino-2-butoxy-8-methoxy-9H-purin-9-yl)methyl]benzyl}piperidin-4-yl)(methyl)amino]ethoxy}phenyl)acetate

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