[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

Base Information

Chemical Name:[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester
CAS No.:556810-27-6
Molecular Formula:C₃₄H₃₈Cl₃NO₃
Molecular Weight:615.04
Hs Code.:

Synonyms:[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

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Chemical Property of [3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

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Technology Process of [3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

There total 3 articles about [3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 112-43-6
10-Undecen-1-ol

: 556810-24-3
[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid methyl ester

: 556810-27-6
[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

Guidance literature:: With 1,3-dichlorotetrabutyldistannoxane; In toluene; for 1h; Heating;
DOI:10.1021/ol0344927

Reference yield:

: 2168-06-1
3,3,3-Tris(4-chlorophenyl)-propionic acid

: 556810-27-6
[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / oxalyl chloride / toluene / 24 h / 20 °C

2: 79 percent / triethylamine / CH₂Cl₂ / 18 h

3: 95 percent / bis(dibutylchlorotin)oxide / toluene / 1 h / Heating

With oxalyl dichloride; 1,3-dichlorotetrabutyldistannoxane; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ol0344927

Reference yield:

: 2172-49-8
3,3,3-tris(4-chlorophenyl)propanoyl chloride

: 556810-27-6
[3,3,3-tris-(4-chloro-phenyl)-propionylamino]-acetic acid undec-10-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / triethylamine / CH₂Cl₂ / 18 h

2: 95 percent / bis(dibutylchlorotin)oxide / toluene / 1 h / Heating

With 1,3-dichlorotetrabutyldistannoxane; triethylamine; In dichloromethane; toluene;
DOI:10.1021/ol0344927