2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide

Base Information

• Chemical Name: 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide
• CAS No.: 130150-31-1
• Molecular Formula: C₁₇H₂₆N₂O₃
• Molecular Weight: 306.405

Synonyms:2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide

Chemical Property of 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide

Chemical Property:

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Technology Process of 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide

There total 5 articles about 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-((3S,4R)-1-Benzyl-3-methyl-piperidin-4-yl)-2-methoxy-N-(2-methoxy-phenyl)-propionamide (130150-22-0) → 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide (130150-31-1)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethanol; under 2585.7 Torr;

DOI:10.1021/jm00172a032

Reference yield:

1-Benzyl-3-methyl-4-piperidon (34737-89-8) → 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide (130150-31-1)

Guidance literature:

Multi-step reaction with 4 steps

1: p-toluenesulfonic acid / toluene / Heating

2: NaBH₄ / methanol / Ambient temperature

3: CH₂Cl₂

4: H₂ / 10percent Pd(OH)2/C / ethanol / 2585.7 Torr

With sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; palladium dihydroxide; In methanol; ethanol; dichloromethane; toluene;

DOI:10.1021/jm00172a032

Reference yield:

2-methoxy-phenylamine (90-04-0) → 2-Methoxy-N-(2-methoxy-phenyl)-N-((3S,4R)-3-methyl-piperidin-4-yl)-propionamide (130150-31-1)

Guidance literature:

Multi-step reaction with 4 steps

1: p-toluenesulfonic acid / toluene / Heating

2: NaBH₄ / methanol / Ambient temperature

3: CH₂Cl₂

4: H₂ / 10percent Pd(OH)2/C / ethanol / 2585.7 Torr

With sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; palladium dihydroxide; In methanol; ethanol; dichloromethane; toluene;

DOI:10.1021/jm00172a032

upstream raw materials:

N-((3S,4R)-1-Benzyl-3-methyl-piperidin-4-yl)-2-methoxy-N-(2-methoxy-phenyl)-propionamide

1-Benzyl-3-methyl-4-piperidon

2-methoxy-phenylamine

[1-Benzyl-3-methyl-piperidin-(4E)-ylidene]-(2-methoxy-phenyl)-amine

Downstream raw materials:

2-Methoxy-N-(2-methoxy-phenyl)-N-[(3S,4R)-3-methyl-1-(2-thiophen-2-yl-ethyl)-piperidin-4-yl]-propionamide

N-{(3S,4R)-1-[2-(4-Ethyl-5-oxo-4,5-dihydro-tetrazol-1-yl)-ethyl]-3-methyl-piperidin-4-yl}-2-methoxy-N-(2-methoxy-phenyl)-propionamide

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