Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate

Base Information Edit

Chemical Name:Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate
CAS No.:139190-68-4
Molecular Formula:C₂₂H₂₈O₄Si
Molecular Weight:384.547
Hs Code.:
Mol file:139190-68-4.mol

Synonyms:Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate Edit

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Technology Process of Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate

There total 2 articles about Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81703-93-7
methyl (2E)-3-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]acrylate

: 139190-68-4
Methyl (4S,E)-5-tert-butyldiphenylsiloxy-4-hydroxy-2-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1: AcOH / H₂O / 19 h / Ambient temperature

2: DMAP, imidazole / dimethylformamide / 16 h / Ambient temperature

With 1H-imidazole; dmap; acetic acid; In water; N,N-dimethyl-formamide;
DOI:10.1055/s-1991-28396