3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

Base Information

Chemical Name:3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid
CAS No.:1064442-02-9
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

Synonyms:3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

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Chemical Property of 3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

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Technology Process of 3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

There total 5 articles about 3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1391999-66-8
benzyl 3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoate

: 1064442-02-9
3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In ethanol; for 3h; Inert atmosphere;
DOI:10.1039/c2ob25273b

Reference yield:

: 1391999-64-6
benzyl 3-hydroxy-5-isopropoxybenzoate

: 1064442-02-9
3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 90 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25273b

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1064442-02-9
3-(2-(tert-butoxy)-2-oxoethoxy)-5-isopropoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 90 °C / Inert atmosphere

2: 5%-palladium/activated carbon; hydrogen / ethanol / 3 h / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1039/c2ob25273b