N-trifluoroacetyl-5-bromoanthranilic acid

Base Information

• Chemical Name: N-trifluoroacetyl-5-bromoanthranilic acid
• CAS No.: 341521-24-2
• Molecular Formula: C₉H₅BrF₃NO₃
• Molecular Weight: 312.043

Synonyms:N-trifluoroacetyl-5-bromoanthranilic acid

Chemical Property of N-trifluoroacetyl-5-bromoanthranilic acid

Chemical Property:

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Technology Process of N-trifluoroacetyl-5-bromoanthranilic acid

There total 1 articles about N-trifluoroacetyl-5-bromoanthranilic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Bromo-2-aminobenzoic acid (5794-88-7) + trifluoroacetic anhydride (407-25-0) → N-trifluoroacetyl-5-bromoanthranilic acid (341521-24-2)

Guidance literature:

at 20 ℃; for 1h;

DOI:10.1021/ma051280b

Reference yield: 65.0%

methylmagnesium bromide (75-16-1) + N-trifluoroacetyl-5-bromoanthranilic acid (341521-24-2) → N-(2-acetyl-4-bromo-phenyl)-2,2,2-trifluoro-acetamide

Guidance literature:

50; In tetrahydrofuran; at 50 ℃;

DOI:10.1016/S0040-4039(01)00160-5

Reference yield: 56.0%

octylmagnesium bromide (17049-49-9) + N-trifluoroacetyl-5-bromoanthranilic acid (341521-24-2) → N-(trifluoroacetyl)-5-bromo-3-nonanoylaniline (870783-24-7)

Guidance literature:

In tetrahydrofuran; diethyl ether; for 24h; Heating;

DOI:10.1021/ma051280b

upstream raw materials:

5-Bromo-2-aminobenzoic acid

trifluoroacetic anhydride

Downstream raw materials:

N-(trifluoroacetyl)-5-bromo-3-nonanoylaniline

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