7-O-benzoylhesperetin

Base Information

Chemical Name:7-O-benzoylhesperetin
CAS No.:1237478-97-5
Molecular Formula:C₂₃H₁₈O₇
Molecular Weight:406.392
Hs Code.:

Synonyms:7-O-benzoylhesperetin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-O-benzoylhesperetin

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Technology Process of 7-O-benzoylhesperetin

There total 1 articles about 7-O-benzoylhesperetin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 520-33-2,41001-90-5,69097-99-0
(S)-2,3-dihydro-5,7-dihydroxy-2-(3-hydroxy-4-methoxyphenyl)-4-benzopyrone

: 98-88-4
benzoyl chloride

: 1237478-97-5
7-O-benzoylhesperetin

Guidance literature:: With pyridine; at 20 ℃; Cooling with ice;
DOI:10.1021/jf1010403

Reference yield: 50.0%

: 1237478-97-5
7-O-benzoylhesperetin

: methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucuronate

: 1237479-01-4
7-O-benzoylhesperetin 3'-O-[methyl (2'',3'',4''-tri-O-acetyl)-β-D-glucopyranosyl uronate]

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; Molecular sieve; Inert atmosphere; Cooling with ice;
DOI:10.1021/jf1010403

Reference yield:

: 1237478-97-5
7-O-benzoylhesperetin

: methyl 2,3,4-tri-O-acetyl-1-O-(trichloroacetimidoyl)-α-D-glucuronate

: 1237479-05-8
hesperetin 3'-O-β-D-glucuronide

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Molecular sieve; Inert atmosphere; Cooling with ice

2.1: water; sodium carbonate / 5 h / 0 - 20 °C / Inert atmosphere

2.2: Dowex 50WX₄-50 H(+) form / pH Ca_. 6 / Inert atmosphere

With boron trifluoride diethyl etherate; water; sodium carbonate; In dichloromethane;
DOI:10.1021/jf1010403