trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

Base Information

Chemical Name:trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate
CAS No.:211995-96-9
Molecular Formula:C₁₅H₂₆O₂
Molecular Weight:238.37
Hs Code.:

Synonyms:trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

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Chemical Property of trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

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Technology Process of trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

There total 4 articles about trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 211995-87-8
trans-4-(pivaloyloxymethyl)cyclohexanecarbaldehyde

: 1754-88-7
ethylenetriphenylphosphorane

: 211995-96-9
trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

Guidance literature:: In tetrahydrofuran; hexane; at 0 - 20 ℃; for 22h;
DOI:10.1246/bcsj.71.1639

Reference yield:

: 3236-48-4
trans-1,4-Cyclohexanedimethanol

: 211995-96-9
trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / pyridine / 2 h / 0 °C

2: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

3: 93 percent / tetrahydrofuran; hexane / 22 h / 0 - 20 °C

With pyridine; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; hexane; dichloromethane; 1: Esterification / 2: Swern oxidation / 3: Wittig reaction;
DOI:10.1246/bcsj.71.1639

Reference yield:

: 19145-96-1
diethyl cyclohexane-trans-1,4-dicarboxylate

: 211995-96-9
trans-4-[(Z)-prop-1-en-1-yl]cyclohexylmethyl pivaloate

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / LiAlH₄ / diethyl ether / 20 °C

2: 61 percent / pyridine / 2 h / 0 °C

3: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / -60 - 20 °C

4: 93 percent / tetrahydrofuran; hexane / 22 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 1: Reduction / 2: Esterification / 3: Swern oxidation / 4: Wittig reaction;
DOI:10.1246/bcsj.71.1639