(pentamethylcyclopentadienyl)2U(benzyl)2

Base Information

Chemical Name:(pentamethylcyclopentadienyl)2U(benzyl)2
CAS No.:79301-24-9
Molecular Formula:C₃₄H₄₄U
Molecular Weight:690.752
Hs Code.:

Synonyms:(pentamethylcyclopentadienyl)2U(benzyl)2

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Chemical Property of (pentamethylcyclopentadienyl)2U(benzyl)2

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Technology Process of (pentamethylcyclopentadienyl)2U(benzyl)2

There total 1 articles about (pentamethylcyclopentadienyl)2U(benzyl)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 67506-89-2
bis(pentamethylcyclopentadienyl)dichlorouranium(IV)

: benzyllithium*2THF

: 79301-24-9
(pentamethylcyclopentadienyl)2U(benzyl)2

Guidance literature:: In diethyl ether; stirred under vac. for 10 min at -78°C; allowed to warm from -78°C to room temp., after 1.5 h evapd., stirred with toluene for 15 min, filtrated, washed with toluene, filtratedfrom cold pentan solution, evapd., dried in vac., elem. anal.;
DOI:10.1021/ja00412a021

Reference yield: 88.0%

: 775342-81-9,79301-24-9
(pentamethylcyclopentadienyl)2U(benzyl)2

: 100-47-0
benzonitrile

: 775342-83-1
(pentamethylcyclopentadienyl)2U[-N=C(Ph)(benzyl)]2

Guidance literature:: In toluene; (N2 or He); addn. of benzonitrile to a soln. of uranium complex in toluene, stirring at room temp. for 12 h; filtration through Celite pad, evapn., recrystn. (toluene, -30°C); elem. anal.;
DOI:10.1021/om0343824

Reference yield: 61.0%

: 79301-24-9
(pentamethylcyclopentadienyl)2U(benzyl)2

: 81874-54-6
2,6-bis(2-pyridinyl)-pyridine-4-carbonitrile

: 108-88-3,15644-74-3,16713-13-6
toluene

: [(C₅Me₅)2U(N=C(CH₂C₆H₅)-2,2':6',2''-terpyridine)2]*0.5C₇H₈

Guidance literature:: In toluene; (N2); std. Schlenk technique; terpyridine was slowly added to soln. of Ucomplex in toluene; stirred at ambient temp. for 14 h; filtered through Celite; concd.; layered with hexane; kept at -30°C; washed (hexane); dried (vac.); elem. anal.;
DOI:10.1021/ic9024475