methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

Base Information

Chemical Name:methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide
CAS No.:497178-06-0
Molecular Formula:C₂₂H₃₂N₂O₉S
Molecular Weight:500.57
Hs Code.:

Synonyms:methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

Suppliers and Price of methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

There total 3 articles about methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 153527-38-9
methyl 3,4-di-O-acetyl-6-S-acetyl-2-benzamido-2-deoxy-6-thio-α-D-glucopyranoside

: 497178-06-0
methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / aq. H₂O₂ / acetic acid / 12 h / 40 °C

2: 4 Angstroem molecular sieves; SO₂Cl₂ / CH₂Cl₂ / 4 h / 20 °C

3: 59 mg / CH₂Cl₂ / -15 °C / pH 6 - 7

With sulfuryl dichloride; 4 A molecular sieve; dihydrogen peroxide; In dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(02)00874-8

Reference yield:

: tetrabutylammonium methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-sulfonate

: 497178-06-0
methyl 3,4-di-O-acetyl-2-benzamido-2,6-dideoxy-α-D-glucopyranoside-6-N-butylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 4 Angstroem molecular sieves; SO₂Cl₂ / CH₂Cl₂ / 4 h / 20 °C

2: 59 mg / CH₂Cl₂ / -15 °C / pH 6 - 7

With sulfuryl dichloride; 4 A molecular sieve; In dichloromethane;
DOI:10.1016/S0040-4020(02)00874-8