benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate

Base Information

Chemical Name:benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate
CAS No.:300667-79-2
Molecular Formula:C₁₉H₁₇N₃O₅
Molecular Weight:367.361
Hs Code.:

Synonyms:benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate

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Chemical Property of benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate

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Technology Process of benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate

There total 2 articles about benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 5396-89-4
benzyl acetoacetate

: 99-61-6
3-nitro-benzaldehyde

: 57-13-6
urea

: 300667-79-2
benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate

Guidance literature:: With para-dodecylbenzenesulfonic acid; at 100 ℃; for 0.166667h; neat (no solvent);
DOI:10.1016/j.cclet.2010.12.030

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 300667-79-2
benzyl 1,2,3,4-tetrahydro-6-methyl-4-(3-nitrophenyl)-2-oxopyrimidine-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-1,3-cyclohexadiene / Reflux

2: cobalt hydrogen sulfate / ethanol / Reflux

With cobalt hydrogen sulfate; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol;
DOI:10.1002/cbdv.201700502