(4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

Base Information

Chemical Name:(4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one
CAS No.:1235303-63-5
Molecular Formula:C₃₁H₃₇NO₇
Molecular Weight:535.637
Hs Code.:

Synonyms:(4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

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Chemical Property of (4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

Chemical Property:

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Technology Process of (4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

There total 1 articles about (4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₁H₃₅NO₇

: 1235303-65-7
(4R,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

: 1235303-63-5
(4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at -78 ℃; for 0.5h; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/chem.200903490

Reference yield: 85.0%

: 1235303-63-5
(4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one

: 100-39-0
benzyl bromide

: 1235303-70-4
(4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-benzyloxypyrrolidin-2-one

Guidance literature:: (4S,5S)-1-(4-methoxybenzyl)-5-[(1S,3S)-4-(4-methoxybenzyloxy)-3-benzyloxy-1-hydroxybutyl]-4-hydroxypyrrolidin-2-one; With sodium hydride; In tetrahydrofuran; mineral oil; at -30 ℃; for 0.5h;

benzyl bromide; With tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 15h;
DOI:10.1002/chem.200903490