2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

Base Information

Chemical Name:2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate
CAS No.:1294368-44-7
Molecular Formula:C₂₃H₂₇BrN₂O₄
Molecular Weight:475.382
Hs Code.:

Synonyms:2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

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Chemical Property of 2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

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Technology Process of 2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

There total 3 articles about 2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 64904-47-8
2-benzoyloxyacetaldehyde

: 5465-63-4
2-bromobenzylamine hydrochloride

: 64-19-7,77671-22-8
acetic acid

: 1294368-44-7
2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

Guidance literature:: With triethylamine; In methanol; at 20 - 50 ℃; Inert atmosphere; Microwave irradiation; Combinatorial reaction / High throughput screening (HTS);
DOI:10.1016/j.tetlet.2011.01.122

Reference yield: 39.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 3959-05-5
2-bromobenzylamine

: 64904-47-8
2-benzoyloxyacetaldehyde

: 64-19-7,77671-22-8
acetic acid

: 1294368-44-7
2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

Guidance literature:: In methanol; for 12h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2017.09.005

Reference yield:

: 101268-52-4
(benzoyloxy)acetaldehyde diethyl acetal

: 1294368-44-7
2-(N-(2-bromobenzyl)acetamido)-3-(tert-butylamino)-3-oxopropyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid; water / 4 h / 20 °C

2: methanol / 12 h / Inert atmosphere; Reflux

With formic acid; water; In methanol; 2: |Ugi Condensation;
DOI:10.1016/j.tet.2017.09.005