6-(3′,4′,5′-trimethoxyphenyl)fulvene

Base Information

Chemical Name:6-(3′,4′,5′-trimethoxyphenyl)fulvene
CAS No.:861907-33-7
Molecular Formula:C₁₅H₁₆O₃
Molecular Weight:244.29
Hs Code.:

Synonyms:6-(3′,4′,5′-trimethoxyphenyl)fulvene

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Chemical Property of 6-(3′,4′,5′-trimethoxyphenyl)fulvene

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Technology Process of 6-(3′,4′,5′-trimethoxyphenyl)fulvene

There total 1 articles about 6-(3′,4′,5′-trimethoxyphenyl)fulvene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 861907-33-7
6-(3′,4′,5′-trimethoxyphenyl)fulvene

Guidance literature:: With pyrrolidine; Inert atmosphere; Schlenk technique;
DOI:10.1002/aoc.3117

Reference yield: 66.0%

: 861907-33-7
6-(3′,4′,5′-trimethoxyphenyl)fulvene

: 7550-45-0
titanium tetrachloride

: ansa-[1,2-di(cyclopentadienyl)-1,2-di(3',4',5'-trimethoxyphenyl)ethandeiyl]titanium dichloride

Guidance literature:: In tetrahydrofuran; toluene; under Ar, 1 M TiCl4 in toluene was added to 9:1 (v/v) toluene-THF mixt.,nBuLKi was added at -78 °C, 20 h stirring at room temp., alkene was added in toluene at room temp., reflux for 16 h; solvent was removed in vac., solid 3 times extd. with CHCl3, soln. was filtered via Celite, solvent was removed in vac., dissoln. in CHCl3, filtration via Whatman No.1. paper,, evapn. in vac., trituration with pentane, elem. anal.; 58:42 cis:trans ratio;
DOI:10.1016/j.poly.2005.02.017

Reference yield: 52.0%

: NbCl₄(THF)₂

: 861907-33-7
6-(3′,4′,5′-trimethoxyphenyl)fulvene

: 1577229-49-2
C₃₀H₃₄Cl₂NbO₆

Guidance literature:: 6-(3′,4′,5′-trimethoxyphenyl)fulvene; With lithium triethylborohydride; In tetrahydrofuran; diethyl ether; Inert atmosphere; Schlenk technique;

NbCl₄(THF)₂; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/aoc.3117