C₁₄H₁₅N

Base Information

Chemical Name:C₁₄H₁₅N
CAS No.:1294513-60-2
Molecular Formula:C₁₄H₁₅N
Molecular Weight:197.28
Hs Code.:

Synonyms:C₁₄H₁₅N

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Chemical Property of C₁₄H₁₅N

Chemical Property:

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Technology Process of C₁₄H₁₅N

There total 7 articles about C₁₄H₁₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1294513-59-9
AcNHPhDN

: 1294513-60-2
C₁₄H₁₅N

Guidance literature:: With water; potassium hydroxide; In ethanol; at 80 ℃; for 12h;

Reference yield:

: 1165952-91-9
cyclohexa-1,3-diene

: 1294513-60-2
C₁₄H₁₅N

Guidance literature:: Multi-step reaction with 5 steps

1.1: 3,5-dibutyl-4-hydroxytoluene / 40 h / 70 °C / Inert atmosphere

2.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; oxygen / dichloromethane; water / 40 h / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.2: 48 h / 20 °C

4.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 2 h / Inert atmosphere; Reflux

5.1: potassium hydroxide; water / ethanol / 12 h / 80 °C

With 3,5-dibutyl-4-hydroxytoluene; water; oxygen; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; potassium hydroxide; sodium hydroxide; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; 4.1: Suzuki Coupling;

Reference yield:

: (+/-)-bicyclo[2.2.2]oct-5-ene-2-carboxylic acid benzyl ester

: 1294513-60-2
C₁₄H₁₅N

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide; water / ethanol / 12 h / 20 °C / Inert atmosphere

1.2: pH 1

2.1: lithium diisopropyl amide / N,N,N,N,N,N-hexamethylphosphoric triamide; tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

3.1: N,N-dimethyl-formamide dimethyl acetal / dichloromethane / 12 h / -78 - 20 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.2: 48 h / 20 °C

5.1: sodium hydrogencarbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 2 h / Inert atmosphere; Reflux

6.1: potassium hydroxide; water / ethanol / 12 h / 80 °C

With water; sodium hydrogencarbonate; N,N-dimethyl-formamide dimethyl acetal; potassium hydroxide; sodium hydroxide; lithium diisopropyl amide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; dichloromethane; toluene; 5.1: Suzuki Coupling;