C₅₆H₇₈N₄O₁₂

Base Information

• Chemical Name: C₅₆H₇₈N₄O₁₂
• CAS No.: 1613643-87-0
• Molecular Formula: C₅₆H₇₈N₄O₁₂
• Molecular Weight: 999.255
• Mol file: 1613643-87-0.mol

Synonyms:C₅₆H₇₈N₄O₁₂

Chemical Property of C₅₆H₇₈N₄O₁₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₆H₇₈N₄O₁₂

There total 3 articles about C₅₆H₇₈N₄O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3'-dibromobiphenyl (16400-51-4) + C28H47BN2O8 (1382469-17-1) → C56H78N4O12 (1613643-87-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; at 20 - 104 ℃; for 4.5h; Inert atmosphere; Microwave irradiation;

Reference yield:

C22H35BrN2O6 (1382469-16-0) → C56H78N4O12 (1613643-87-0)

Guidance literature:

Multi-step reaction with 2 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 20 - 80 °C / Inert atmosphere

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 4.5 h / 20 - 104 °C / Inert atmosphere; Microwave irradiation

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; potassium carbonate; In 1,4-dioxane; dimethyl sulfoxide;

Reference yield:

(3-bromophenyl)boronic acid (89598-96-9) → C56H78N4O12 (1613643-87-0)

Guidance literature:

Multi-step reaction with 2 steps

1: copper diacetate / 1,2-dichloro-ethane / 1 h / 100 °C

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 4.5 h / 20 - 104 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper diacetate; potassium carbonate; In 1,4-dioxane; 1,2-dichloro-ethane;

upstream raw materials:

C₂₂H₃₅BrN₂O₆

3,3'-dibromobiphenyl

C₂₈H₄₇BN₂O₈

(3-bromophenyl)boronic acid

Downstream raw materials:

C₃₆H₄₆N₄O₄