4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine

Base Information

• Chemical Name: 4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine
• CAS No.: 167143-43-3
• Molecular Formula: C₂₅H₃₃NO₅
• Molecular Weight: 427.541

Synonyms:4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine

Chemical Property of 4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine

Chemical Property:

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Technology Process of 4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine

There total 1 articles about 4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[2-(3-methoxyphenyl)ethyl]phenol (167145-13-3) + 4-t-butoxycarbonyl-2-[(4-methylphenylsulphonyloxy)methyl]morpholine (130546-33-7) → 4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine (167143-43-3)

Guidance literature:

2-[2-(3-methoxyphenyl)ethyl]phenol; With potassium tert-butylate; In N,N-dimethyl acetamide; at 0 ℃; for 0.166667h;

4-t-butoxycarbonyl-2-[(4-methylphenylsulphonyloxy)methyl]morpholine; In N,N-dimethyl acetamide; at 20 ℃;

DOI:10.1248/cpb.48.245

Reference yield: 52.0%

4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine (167143-43-3) → (E)-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine hydrochloride

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; ethyl acetate;

Reference yield:

4-t-butoxycarbonyl-2-{2-[2-(3-methoxyphenyl)ethyl]phenoxymethyl}morpholine (167143-43-3) → 2-{2-[2-(3-methoxy-phenyl)-ethyl]-phenoxymethyl}-4-methyl-morpholine

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2.5h; Heating;

DOI:10.1248/cpb.48.245

upstream raw materials:

2-[2-(3-methoxyphenyl)ethyl]phenol

4-t-butoxycarbonyl-2-[(4-methylphenylsulphonyloxy)methyl]morpholine

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