3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

Base Information

Chemical Name:3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate
CAS No.:1311946-27-6
Molecular Formula:C₁₇H₁₈N₂O₅S
Molecular Weight:362.406
Hs Code.:

Synonyms:3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

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Chemical Property of 3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

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Technology Process of 3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

There total 5 articles about 3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 150-19-6
O-methylresorcine

: 1311946-41-4
4-(tetrahydro-2-oxopyrimidin-1(2H)-yl)benzene-1-sulfonyl chloride

: 1311946-27-6
3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 24h; Inert atmosphere;
DOI:10.1021/jm200488a

Reference yield: 72.0%

: 1311946-27-6
3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

Guidance literature:

Reference yield:

: 56535-85-4
3,4,5,6-tetrahydro-1-phenylpyrimidin-2(1H)-one

: 1311946-27-6
3-methoxyphenyl 4-[tetrahydro-2-oxopyrimidin-1(2H)-yl]benzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / tetrachloromethane / 2 h / 0 °C / Inert atmosphere

2: triethylamine / dichloromethane / 24 h / 25 °C / Inert atmosphere

With chlorosulfonic acid; triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/jm200488a