1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

Base Information

Chemical Name:1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane
CAS No.:960054-47-1
Molecular Formula:C₃₄H₅₉N₅O₈S
Molecular Weight:697.937
Hs Code.:

Synonyms:1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

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Chemical Property of 1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

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Technology Process of 1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

There total 1 articles about 1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 960054-45-9
N-mesitylenesulfonyl aziridine

: 175854-39-4
1,4,7-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

: 960054-47-1
1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

Guidance literature:: In acetonitrile; at 105 ℃;
DOI:10.1039/b709422a

Reference yield: 94.0%

: 960054-47-1
1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane

: 555-77-1
tris-(2-chloro-ethyl)-amine

: tris[3-aza-3-mesitylenesulfonyl-5-{4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododec-1-yl}pentyl]amine

Guidance literature:: 1-(2-mesitylenesulfonylaminoethyl)-4,7,10-tris(tert-butyloxycarbonyl)-1,4,7,10-tetraazacyclododecane; With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃; for 2h;

tris-(2-chloro-ethyl)-amine; In N,N-dimethyl-formamide; at 70 ℃; Further stages.;
DOI:10.1039/b709422a