2,4-dimethyl-1,2,4-triazine-3,5-dione

Base Information

• Chemical Name: 2,4-dimethyl-1,2,4-triazine-3,5-dione
• CAS No.: 15677-10-8
• Molecular Formula: C5H7 N3 O2
• Molecular Weight: 141.13
• Hs Code.: 2933699090
• Mol file: 15677-10-8.mol

Synonyms:as-Triazine-3,5(2H,4H)-dione,2,4-dimethyl- (6CI,7CI,8CI); 1,3-Dimethyl-6-azauracil;2,4-Dimethyl-1,2,4-triazine-3,5(2H)-dione;2,4-Dimethyl-3,5-dioxo-(2H,4H)-1,2,4-triazine; 6-Aza-1,3-dimethyluracil; NSC227396

Chemical Property of 2,4-dimethyl-1,2,4-triazine-3,5-dione

Chemical Property:

• Vapor Pressure: 0.564mmHg at 25°C
• Boiling Point: 189.6°Cat760mmHg
• PKA: -1.76±0.20(Predicted)
• Flash Point: 68.5°C
• PSA: 56.89000
• Density: 1.36g/cm³
• LogP: -1.52100

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-dimethyl-1,2,4-triazine-3,5-dione

There total 3 articles about 2,4-dimethyl-1,2,4-triazine-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

6-azauracil (461-89-2) + methyl iodide (74-88-4) → 6-azido-1,3-dimethyluracil (15677-10-8)

Guidance literature:

6-azauracil; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h;

methyl iodide; In N,N-dimethyl-formamide; for 16h;

DOI:10.3390/molecules21121683

Reference yield:

6-azauracil (461-89-2) → 6-azido-1,3-dimethyluracil (15677-10-8)

Guidance literature:

With CH₃I; NaH; In N,N-dimethyl-formamide; paraffin;

Reference yield:

→ 6-azido-1,3-dimethyluracil (15677-10-8)

Guidance literature:

3,5-Dioxo-2,3,4,5-tetrahydro-1,2,4-triazin, CH3I, wss. Alkali;

upstream raw materials:

6-azauracil

methyl iodide

Downstream raw materials:

4-((3aR,7aS,7bS)-3a,7b-Dichloro-4,6-dimethyl-1,3,5,7-tetraoxo-octahydro-2,3b,4,6-tetraaza-cyclopenta[3,4]cyclobuta[1,2]benzen-2-yl)-benzoic acid ethyl ester

(3aR,7aS,7bS)-3a,7b-Dichloro-2-(3,5-dichloro-phenyl)-4,6-dimethyl-dihydro-2,3b,4,6-tetraaza-cyclopenta[3,4]cyclobuta[1,2]benzene-1,3,5,7-tetraone

8-Azacaffeine

2,4,6-trimethyl-2H-[1,2,3]triazolo[4,5-d]pyrimidine-5,7(4H,6H)-dione