4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

Base Information

Chemical Name:4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol
CAS No.:944389-36-0
Molecular Formula:C₂₅H₃₀O₆
Molecular Weight:426.51
Hs Code.:

Synonyms:4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

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Chemical Property of 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

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Technology Process of 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

There total 10 articles about 4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 944389-34-8
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)but-3-yl-2-ol

: 944389-36-0
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

Guidance literature:: With hydrogen; potassium hydrogencarbonate; palladium on activated charcoal; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.tet.2007.02.033

Reference yield:

: 944389-25-7
2-(2-methoxymethoxy-naphthalen-1-yl)acetaldehyde

: 944389-36-0
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: 76 percent / tetrahydrofuran / -78 - 20 °C

2.1: 83 percent / potassium bicarbonate; hydrogen / palladium on carbon / ethyl acetate / 20 °C

With n-butyllithium; hydrogen; potassium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1016/j.tet.2007.02.033

Reference yield:

: 944389-23-5
1-allyl-2-methoxymethoxy-naphthalene

: 944389-36-0
4-(3-methoxy-2-(methoxymethoxy)phenyl)-1-(2-methoxymethoxy-naphthalen-1-yl)butan-2-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: 72 percent / osmium tetroxide; N-methylmorpholine-N-oxide / acetone; H₂O; 2-methyl-propan-2-ol / 16 h

2.1: 62 percent / sodium periodate / CH₂Cl₂; H₂O / 0.75 h / 20 °C

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

3.2: 76 percent / tetrahydrofuran / -78 - 20 °C

4.1: 83 percent / potassium bicarbonate; hydrogen / palladium on carbon / ethyl acetate / 20 °C

With sodium periodate; osmium(VIII) oxide; n-butyllithium; hydrogen; potassium hydrogencarbonate; 4-methylmorpholine N-oxide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; ethyl acetate; acetone; tert-butyl alcohol;
DOI:10.1016/j.tet.2007.02.033