ethyl [1-(benzyl)piperidin-4-yl]thioacetate

Base Information

Chemical Name:ethyl [1-(benzyl)piperidin-4-yl]thioacetate
CAS No.:741729-83-9
Molecular Formula:C₁₆H₂₃NO₂S
Molecular Weight:293.43
Hs Code.:

Synonyms:ethyl [1-(benzyl)piperidin-4-yl]thioacetate

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Chemical Property of ethyl [1-(benzyl)piperidin-4-yl]thioacetate

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Technology Process of ethyl [1-(benzyl)piperidin-4-yl]thioacetate

There total 2 articles about ethyl [1-(benzyl)piperidin-4-yl]thioacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 105-36-2
ethyl bromoacetate

: 139362-30-4
1-(phenylmethyl)piperidine-4-thiol

: 741729-83-9
ethyl [1-(benzyl)piperidin-4-yl]thioacetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 16h;
DOI:10.1248/cpb.52.675

Reference yield:

: 3612-20-2
1-phenylmethyl-4-piperidone

: 741729-83-9
ethyl [1-(benzyl)piperidin-4-yl]thioacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂S / propan-2-ol / 71 h / 20 °C

1.2: 100 percent / NaBH₄ / propan-2-ol / 1 h / 55 °C

2.1: 69 percent / K₂CO₃ / acetonitrile / 16 h / 20 °C

With hydrogen sulfide; potassium carbonate; In isopropyl alcohol; acetonitrile;
DOI:10.1248/cpb.52.675