4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

Base Information

Chemical Name:4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester
CAS No.:1161418-97-8
Molecular Formula:C₂₃H₂₃Cl₂NO₄S
Molecular Weight:480.412
Hs Code.:

Synonyms:4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

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Chemical Property of 4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

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Technology Process of 4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

There total 3 articles about 4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1161418-96-7
3-{[bis(4-chlorophenyl)methyl]amino}propane-1,2-diol

: 98-59-9
p-toluenesulfonyl chloride

: 1161418-97-8
4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

Guidance literature:: 3-{[bis(4-chlorophenyl)methyl]amino}propane-1,2-diol; p-toluenesulfonyl chloride; With pyridine; In toluene; at -7 - 20 ℃; Inert atmosphere;

In water; toluene;

Reference yield:

: 90-98-2
4,4'-Dichlorobenzophenone

: 1161418-97-8
4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / ethanol; xylene / 20 - 140 °C / Inert atmosphere

2.1: sodium tetrahydroborate / water; xylene / 20 - 102 °C

2.2: 20 - 22 °C

2.3: pH 8 - 9

3.1: pyridine / toluene / -7 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; toluene-4-sulfonic acid; In ethanol; water; toluene; xylene;

Reference yield:

: 1161418-95-6
3-{[bis(4-chlorophenyl)methylene]amino}propane-1,2-diol

: 1161418-97-8
4-toluenesulphonic acid 3-{[bis(4-chlorophenyl)methyl]amino}-2-hydroxypropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / water; xylene / 20 - 102 °C

1.2: 20 - 22 °C

1.3: pH 8 - 9

2.1: pyridine / toluene / -7 - 20 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; In water; toluene; xylene;