ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

Base Information

Chemical Name:ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate
CAS No.:365462-88-0
Molecular Formula:C₃₀H₃₃N₅O₃
Molecular Weight:511.624
Hs Code.:

Synonyms:ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

There total 7 articles about ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 365462-70-0
ethyl 3-amino-4-[(3-cyanophenylamino)methyl]benzoate

: 303134-03-4
4-(4-methyl-1,4-diazepan-1-yl)benzoic acid hydrochloride

: ethyl acetate n-hexane

: 365462-88-0
ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

Guidance literature:: With thionyl chloride; sodium chloride; sodium hydrogencarbonate; In pyridine; chloroform; ethyl acetate;

Reference yield:

: 96315-16-1
4-bromomethyl-3-nitrobenzoic acid ethyl ester

: 365462-88-0
ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 12.63 g / potassium carbonate / acetonitrile / 3 h / 70 °C

2: Fe; ammonium chloride / ethanol; H₂O / 0.5 h / Heating

3: pyridine / 20 h / 20 °C

With pyridine; ammonium chloride; iron; potassium carbonate; In ethanol; water; acetonitrile;
DOI:10.1016/j.bmc.2004.11.005

Reference yield:

: 365462-69-7
ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-nitrobenzoate

: 365462-88-0
ethyl 4-{[(3-cyanophenyl)amino]methyl}-3-{[4-(4-methyl-1,4-diazepan-1-yl)benzoyl]amino}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: Fe; ammonium chloride / ethanol; H₂O / 0.5 h / Heating

2: pyridine / 20 h / 20 °C

With pyridine; ammonium chloride; iron; In ethanol; water;
DOI:10.1016/j.bmc.2004.11.005