3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

Base Information

Chemical Name:3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole
CAS No.:1196103-39-5
Molecular Formula:C₁₆H₁₉F₃N₂O₃S
Molecular Weight:376.4
Hs Code.:

Synonyms:3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

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Chemical Property of 3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

Chemical Property:

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Technology Process of 3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

There total 3 articles about 3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1004770-41-5
2-methyl-2-(4-trifluoromethyl-benzenesulfonyl)-propionic acid chloride

: 42956-75-2
N'-hydroxypivalimidamide

: 1196103-39-5
3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

Guidance literature:: With pyridine; at 110 ℃; for 3h; Molecular sieves;

Reference yield:

: 2-methyl-2-((4-(trifluoromethyl)phenyl)sulfonyl)propanoic acid

: 1196103-39-5
3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: pyridine / 3 h / 110 °C / Inert atmosphere

With pyridine; thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;

Reference yield:

: 630-18-2
tert-butyl isocyanide

: 1196103-39-5
3-tert-butyl-5-[1-methyl-1-(4-trifluoromethyl-benzenesulfonyl)-ethyl]-[1,2,4]oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; hydroxylamine hydrochloride / ethanol; water / 16.5 h / 20 °C / Reflux

2: pyridine / 3 h / 110 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; potassium carbonate; In ethanol; water;