N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

Base Information

Chemical Name:N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine
CAS No.:1311285-35-4
Molecular Formula:C₁₆H₂₁N₃OS
Molecular Weight:303.428
Hs Code.:

Synonyms:N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

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Chemical Property of N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

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Technology Process of N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

There total 2 articles about N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 21553-46-8
4-methoxy-3,5-dimethylbenzoic acid

: 122813-74-5
4-cyclopentyl thiosemicarbazide

: 1311285-35-4
N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: 4-methoxy-3,5-dimethylbenzoic acid; With trichlorophosphate; In 1,4-dioxane; at 90 ℃; for 3h;

4-cyclopentyl thiosemicarbazide; In 1,4-dioxane; at 100 ℃; for 2h;

With sodium hydroxide; In 1,4-dioxane; water; pH=7; Cooling with ice;

Reference yield:

: 33522-03-1
cyclopentyl isothiocyanate

: 1311285-35-4
N-cyclopentyl-5-(4-methoxy-3,5-dimethylphenyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / ethanol / 1.5 h / 20 °C

2.1: trichlorophosphate / 1,4-dioxane / 3 h / 90 °C

2.2: 2 h / 100 °C

2.3: pH 7 / Cooling with ice

With hydrazine hydrate; trichlorophosphate; In 1,4-dioxane; ethanol;