2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Base Information

Chemical Name:2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide
CAS No.:123420-24-6
Molecular Formula:C₃₄H₃₉NO₃P*I
Molecular Weight:667.567
Hs Code.:

Synonyms:2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

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Chemical Property of 2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

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Technology Process of 2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

There total 3 articles about 2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 123420-23-5
2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

: 123420-24-6
2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 9h; Ambient temperature;
DOI:10.1055/s-1989-27232

Reference yield:

: 101-06-4
N,N-dibenzyl-2-aminoethanol

: 123420-24-6
2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / n-BuLi / diethyl ether / 120 h / Ambient temperature

2: 95 percent / H₂, conc. aq. HCl / 10percent Pd/C / methanol / 9 h / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; n-butyllithium; In methanol; diethyl ether;
DOI:10.1055/s-1989-27232

Reference yield:

: 82777-75-1
1-<(2-Methyl-1,3-dioxolan-2-yl)methyl>ethenyltriphenylphosphonium iodide

: 123420-24-6
2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / n-BuLi / diethyl ether / 120 h / Ambient temperature

2: 95 percent / H₂, conc. aq. HCl / 10percent Pd/C / methanol / 9 h / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; n-butyllithium; In methanol; diethyl ether;
DOI:10.1055/s-1989-27232