5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxy^α-26,28-(crown-4)^α-27-hydroxy^α-calix[4]arene

Base Information

• Chemical Name: 5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxy^α-26,28-(crown-4)^α-27-hydroxy^α-calix[4]arene
• CAS No.: 369600-26-0
• Molecular Formula: C₆₀H₇₈O₆
• Molecular Weight: 895.276

Synonyms:5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxy^α-26,28-(crown-4)^α-27-hydroxy^α-calix[4]arene

Chemical Property of 5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxy^α-26,28-(crown-4)^α-27-hydroxy^α-calix[4]arene

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Technology Process of 5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxy^α-26,28-(crown-4)^α-27-hydroxy^α-calix[4]arene

There total 1 articles about 5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxy^α-26,28-(crown-4)^α-27-hydroxy^α-calix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

triethylene glycol di-(p-toluenesulfonate) (19249-03-7) + 5,11,17,23-tetrakis(1,1-dimethylethyl)-25-propoxy-27-benzyloxy-26,28-dihydroxy-calix[4]arene (244177-19-3) → 5,11,17,23-Tetrakis(1,1-dimethylethyl)-25-benzyloxyα-26,28-(crown-4)α-27-hydroxyα-calix[4]arene (369600-26-0)

Guidance literature:

5,11,17,23-tetrakis(1,1-dimethylethyl)-25-propoxy-27-benzyloxy-26,28-dihydroxy-calix[4]arene; With sodium hydride; In tetrahydrofuran; for 4h; Heating;

triethylene glycol di-(p-toluenesulfonate); In tetrahydrofuran; for 20h; Further stages.; Heating;

DOI:10.1002/1521-3765(20010803)7:15<3354::AID-CHEM3354>3.0.CO;2-U

upstream raw materials:

triethylene glycol di-(p-toluenesulfonate)

5,11,17,23-tetrakis(1,1-dimethylethyl)-25-propoxy-27-benzyloxy-26,28-dihydroxy-calix[4]arene

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