2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

Base Information

Chemical Name:2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone
CAS No.:174876-46-1
Molecular Formula:C₃₃H₄₀O₆
Molecular Weight:532.677
Hs Code.:

Synonyms:2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

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Chemical Property of 2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

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Technology Process of 2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

There total 4 articles about 2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 174876-43-8
2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzyl]phenol

: 174876-46-1
2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

Guidance literature:: With potassium hydroxide; potassium hexacyanoferrate(III); In benzene; for 5h;

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 174876-46-1
2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / polyphosphoric acid / 4 h / 80 - 85 °C

2: 82 percent / Mg(ClO₄)2 / CHCl₃ / 6 h / Heating

3: 100 percent / potassium hexacyanoferrate(III), aq. KOH / benzene / 5 h

With potassium hydroxide; PPA; magnesium(II) perchlorate; potassium hexacyanoferrate(III); In chloroform; benzene;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 174876-46-1
2,6-di-tert-butyl-4-[2-(3,4-dimethoxyphenacyl)-4,5-dimethoxybenzylidene]-2,5-cyclohexadienone

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / polyphosphoric acid / 4 h / 80 - 85 °C

2: 82 percent / Mg(ClO₄)2 / CHCl₃ / 6 h / Heating

3: 100 percent / potassium hexacyanoferrate(III), aq. KOH / benzene / 5 h

With potassium hydroxide; PPA; magnesium(II) perchlorate; potassium hexacyanoferrate(III); In chloroform; benzene;