4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

Base Information

Chemical Name:4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide
CAS No.:157465-52-6
Molecular Formula:C₃₄H₃₅NO₅
Molecular Weight:537.656
Hs Code.:

4-(2,2-dimethyl-propionyl)-<i>N</i>-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

Synonyms:4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

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Chemical Property of 4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

Chemical Property:

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Technology Process of 4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

There total 5 articles about 4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: 139681-41-7
4-(2,2-dimethyl-1-oxopropyl)-N-(2-hydroxyethoxy)benzamide

: 157465-52-6
4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1021/jm980438y

Reference yield:

: 30314-44-4
2,2-dimethyl-1-(4-methylphenyl)-1-propanone

: 157465-52-6
4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 56 percent / aq. KMnO₄ / 4 h / Heating

2: 99 percent / SOCl₂ / 1.5 h / Heating

3: 82 percent / hydroxylamine hydrochloride, 2N aq. NaOH / diethyl ether / 0 °C

4: 63 percent / NaOH / ethanol / 24 h / Heating

5: 18.6 g / pyridine / CH₂Cl₂ / 2 h / 0 - 20 °C

With pyridine; sodium hydroxide; potassium permanganate; thionyl chloride; hydroxylamine hydrochloride; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm980438y

Reference yield:

: 32018-31-8
4-pivaloyl-benzoic acid

: 157465-52-6
4-(2,2-dimethyl-propionyl)-N-{2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / SOCl₂ / 1.5 h / Heating

2: 82 percent / hydroxylamine hydrochloride, 2N aq. NaOH / diethyl ether / 0 °C

3: 63 percent / NaOH / ethanol / 24 h / Heating

4: 18.6 g / pyridine / CH₂Cl₂ / 2 h / 0 - 20 °C

With pyridine; sodium hydroxide; thionyl chloride; hydroxylamine hydrochloride; In diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm980438y