C₂₄H₂₆ClN₅O

Base Information

Chemical Name:C₂₄H₂₆ClN₅O
CAS No.:1404555-72-1
Molecular Formula:C₂₄H₂₆ClN₅O
Molecular Weight:435.956
Hs Code.:

C<sub>24</sub>H<sub>26</sub>ClN<sub>5</sub>O

Synonyms:C₂₄H₂₆ClN₅O

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Chemical Property of C₂₄H₂₆ClN₅O

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Technology Process of C₂₄H₂₆ClN₅O

There total 9 articles about C₂₄H₂₆ClN₅O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1404555-71-0
tert-butyl {(3R)-1-[3-(2-chlorobenzyl)-5,7-dimethyl-4-oxo-4,5-dihydro-3H-imidazo[4,5-c]quinolin-2-yl]piperidin-3-yl}carbamate

: 1404555-72-1
C₂₄H₂₆ClN₅O

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 4h;
DOI:10.1016/j.bmc.2012.07.046

Reference yield:

: 853070-06-1
C₃₂H₃₉ClIN₅O₅

: 1404555-72-1
C₂₄H₂₆ClN₅O

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2.1: silver (I) hydrogen carbonate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 150 °C

3.1: hydrogenchloride / 1,4-dioxane / 4 h / 80 °C

4.1: sodium hydrogencarbonate / tetrahydrofuran; water / 3 h / 20 °C

5.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1.5 h / 0 °C

5.2: 5 h / 0 - 20 °C

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 16 h / 20 °C

7.1: sodium tetrahydroborate / dimethyl sulfoxide / 3 h / 50 °C

8.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

With 1H-imidazole; hydrogenchloride; sodium tetrahydroborate; silver (I) hydrogen carbonate; iodine; palladium diacetate; chloroformic acid ethyl ester; sodium hydrogencarbonate; potassium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.07.046

Reference yield:

: 853069-86-0
methyl 3-[{[2-{(3R)-3-[(tert-butoxycarbonyl)amino]piperidin-1-yl}-1-(2-chlorobenzyl)-4-iodo-1H-imidazol-5-yl]carbonyl}(methyl)amino]benzoate

: 1404555-72-1
C₂₄H₂₆ClN₅O

Guidance literature:: Multi-step reaction with 7 steps

1.1: silver (I) hydrogen carbonate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 150 °C

2.1: hydrogenchloride / 1,4-dioxane / 4 h / 80 °C

3.1: sodium hydrogencarbonate / tetrahydrofuran; water / 3 h / 20 °C

4.1: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 1.5 h / 0 °C

4.2: 5 h / 0 - 20 °C

5.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 16 h / 20 °C

6.1: sodium tetrahydroborate / dimethyl sulfoxide / 3 h / 50 °C

7.1: hydrogenchloride / 1,4-dioxane / 4 h / 20 °C

With 1H-imidazole; hydrogenchloride; sodium tetrahydroborate; silver (I) hydrogen carbonate; iodine; palladium diacetate; chloroformic acid ethyl ester; sodium hydrogencarbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.07.046