C₃₁H₂₅IO₃

Base Information

Chemical Name:C₃₁H₂₅IO₃
CAS No.:1416152-51-6
Molecular Formula:C₃₁H₂₅IO₃
Molecular Weight:572.442
Hs Code.:

C<sub>31</sub>H<sub>25</sub>IO<sub>3</sub>

Synonyms:C₃₁H₂₅IO₃

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Chemical Property of C₃₁H₂₅IO₃

Chemical Property:

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Technology Process of C₃₁H₂₅IO₃

There total 5 articles about C₃₁H₂₅IO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1416152-50-5
C₃₂H₂₆O₅

: 1416152-51-6
C₃₁H₂₅IO₃

Guidance literature:: C₃₂H₂₆O₅; With diphenyl phosphoryl azide; triethylamine; In ethanol; toluene; at 20 - 70 ℃; for 4h;

With potassium hydroxide; In ethanol; toluene; for 3h; Reflux;

With hydrogenchloride; potassium iodide; sodium nitrite; In water; acetonitrile; at 5 - 20 ℃; for 3h;

Reference yield:

: 116413-49-1
(3-bromo-4-methoxyphenyl)-phenylmethanone

: 1416152-51-6
C₃₁H₂₅IO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane; ethanol / 3 h / 78 °C

2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 55 °C

2.2: 2 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C

4.1: triethylamine; diphenyl phosphoryl azide / toluene; ethanol / 4 h / 20 - 70 °C

4.2: 3 h / Reflux

4.3: 3 h / 5 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; potassium tert-butylate; sodium carbonate; potassium carbonate; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 5720-07-0
4-methoxyphenylboronic acid

: 1416152-51-6
C₃₁H₂₅IO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane; ethanol / 3 h / 78 °C

2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 55 °C

2.2: 2 h / Reflux

3.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 60 °C

4.1: triethylamine; diphenyl phosphoryl azide / toluene; ethanol / 4 h / 20 - 70 °C

4.2: 3 h / Reflux

4.3: 3 h / 5 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; diphenyl phosphoryl azide; potassium tert-butylate; sodium carbonate; potassium carbonate; triethylamine; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide; toluene;